The reconstruct of the stick-slip and creep histories is essential for understanding fault activities and seismic hazard assessment. Distinguishing stick-slip and creep using geodetic technology has become a hot research area in recent years, but distinguishing and estimating seismic slip and creep on geological timescales(e.g., over hundreds of years)is challenging due to the lack of historical, geodetic and remote sensing data extending back more than a few hundred years. This study uses a newly developed dating technique(rock surface optically-stimulated-luminescence(OSL)dating)combined with the OSL decay parameters of granite samples from the Langshan fault in Inner Mongolia to simulate optically stimulated OSL-depth curves and depths of half saturation of luminescence signal under various scenarios such as fault seismic slipping, creeping, and erosion of colluvial wedge. The study compares these OSL-depth profiles, especially the depths of the half saturation, under different slipping modes, and summarizes their features.
During fault seismic slip, samples at different heights along the fault scarp display a “step-like” distribution pattern at their depths of half saturation. While during creep, however, they exhibit a “slope-like” pattern. Such differences may lie in that the slope during accelerating creeping is steeper than the slope during constant-speed creeping. Correspondingly, the resolution of residual luminescence-depth profile and depth of half saturation is also higher during accelerating creeping. During intra-earthquake creep events between seismic slip occurrences on the bedrock fault scarp, the distribution of half-saturation depth in the samples includes segments resembling both “steps” and “slopes”, which indicate the seismic slip and creep activities of the fault respectively. If the samples at the base of the colluvial wedge have had a sufficiently long last exposure time, the luminescence-depth profile and half-saturation depth distribution due to the erosion of the colluvial wedge would be approximately the same as in the three-phase seismic slip scenario. This indicates that samples previously buried by the colluvial wedge may be considered within the seismic displacement. Conversely, if the last exposure time of the base samples at the base of the colluvial wedge is short, the bleaching depth of the luminescence signal of these base samples will be noticeably shallower than that of the other samples within the seismic displacement, indicating the observed erosion of the colluvial wedge in this case. Furthermore, the seismic displacement ideally should include the buried location of the colluvial wedge. Therefore, when the luminescence curves and half-saturation depth distributions fail to identify the presence of the colluvial wedge, it is acceptable to include the buried location of the colluvial wedge in the seismic displacement calculation. Conversely, the luminescence-depth curves and half-saturation depth distributions document the erosion caused by the colluvial wedge. The simulation results demonstrate that this method can effectively distinguish between fault slipping and creeping, obtain corresponding displacements, and potentially record the erosion of colluvial wedge.
This study also analyzes the temporal resolution of the method for distinguishing fault activity times and the spatial resolution for quantifying displacements. The specific situation is as follows. When exposure age of the bedrock fault scarp is within a thousand years, the rock surface OSL dating method can easily distinguish types of active slips and seismic displacements for the earthquakes with a recurrence interval of hundreds of years. When exposure age of the bedrock fault scarp is in the range of 100-101ka, the method can easily distinguish types of active slips and seismic displacements for the earthquakes with a recurrence interval exceeding a thousand years. When exposure age of the bedrock fault scarp is over ten-thousand years, the resolution of this method may be significantly reduced. The spatial resolution of seismic displacements using this method depends on interval between sampling and testing samples, typically in 10~30cm.
Phytoliths have shown a lot of advantages in dating due to their widespread distribution, structural stability, and preservation integrity, especially since phytolith carbon was used in radiocarbon dating. However, there is a problem of overestimation of phytolith carbon 14C ages, which may be due to its structure destruction during pre-treatment processes of the rapid oxidation and high temperature. It is necessary to identify the subtle changes in its structure under high-temperature conditions based on its chemical composition and certain physical properties. As a special amorphous hydrated SiO2, using their luminescence signals for thermoluminescence(TL)or optically stimulated luminescence(OSL)dating can be directly compared with their 14C ages even as an alternative dating method, and the luminescence property changes of phytoliths may have a reference value for identifying the physical structure changes. In this paper, modern phytolith samples extracted from dry rice straw were taken as an example to study the stability of OSL and isothermal TL(ITL)signals. We conducted a series of conditional experiments to determine the specific experimental process of OSL and ITL165 signals, and discussed the feasibility and reliability of the dose-signal response relationship and test process under different given doses of dose recovery experiments. Moreover, the OSL signal were tested by a conventional single-aliquot regenerative-dose(SAR)protocol which firstly preheated at 200℃/180℃ to remove the instability signal and then blue excited at 125℃. The OSL signal of phytolith sample rapidly decays under blue light and is basically reset within 5s of excitation. The sensitivity corrected OSL signal intensity and regeneration dose can respond one by one and a growth curve can be established, indicating that there is also a trap structure within the phytolith particles that can generate relatively stable OSL signals. However, there are still some problems which need further to be solved such as relatively weak signal intensity and poor sensitivity. The results of bleaching experiment show that the OSL signal intensity of phytolith particles decays exponentially under sunlight, and the OSL signal irradiated by given dose of 85Gy can be bleached about 90%within 100s and bleached completely around 800s, which suggests that the phytolith samples have good sunlight bleaching susceptibility. There is a stable and easily bleached OSL signal in natural phytolith particles, however, the experimental procedure is only suitable for samples with lower given doses(below about 200Gy)and the dose recovery rate of older samples is lower. On the other hand, 425℃ TL peaks were found in the ITL500 curves of phytolith at both a higher given dose(850Gy)and a lower given dose(85Gy), but they could not be used for dating because of instability. There was a remarkble and stable TL peak at 165℃ under a higher given dose(850Gy). The relatively stable ITL165 signal has the potential to be used in dating research and its experimental procedure is also by SAR method. The dose recovery rate of ITL165 signal under different given doses(above about 50Gy)was in the range of 0.8-1.2. Both OSL and ITL165 signals have the potential to be used in dating studies but need to be tested with samples of known-age. The characteristic dose D0 of OSL and ITL165 signals of phytoliths are(326.8±19.5)Gy and(504.9±49.9)Gy, which implys that phytoliths have a greater saturation level than quartzes. Meanwhile, the ITL500 curve heated at different annealing temperatures has the potential to identify changes in phytolith luminescence properties and physical structure. The structure of phytoliths begins to change at around 300-350℃, and irreversible structural changes have occurred at around 600℃ and gradually become sensitized. This also means that the extraction process of phytoliths using wet ashing rather than dry ashing may destroy the structural integrity of phytoliths and resulting in an overestimation of phytolith carbon AMS 14C ages. Whether it is by using AMS 14C dating method or OSL/TL dating method which phytoliths as the main dating material, phytolith particles should not be placed in a high temperature environment above 300℃ at any stage during the experiment in order to avoid irreversible damage to its structure. The luminescence age obtained by the OSL signal and ITL165 signal of phytoliths can be compared with the 14C age to determine whether there exists an overestimation, and if the two ages can be verified, there is no need to use other dating minerals which is of great significance for the dating of precious archaeological materials.
Terrestrial in-situ cosmogenic nuclide dating(TCND)is one of the most important geochronological techniques for the paleoseismic study of bedrock fault scarps, landslides, and rock avalanches. With many target minerals, due to its uncomplicated composition, widespread occurrence, and simple chemical treatment, Quartz has emerged as an ideal dating material for terrestrial in-situ cosmogenic nuclides dating methods, such as 14C, 10Be, 21Ne, and 26A1. Prior to accelerator mass spectrometry measurement, the separation of pure quartz from field-collected rock samples was a pivotal step in TCND. However, the elevated aluminum content in quartz samples undermines the reliability of TCND results. Generally, most of the aluminum content in samples originates from impurities like feldspar. To ensure accurate dating outcomes, the content of Al in samples should be reduced to less than 200 ppm. Therefore, effective separation of feldspar and quartz in samples and obtaining pure quartz is the first step in TCN dating. The conventional HF/HNO3 etching method to separate and purify quartz is widely utilized, but it is time-consuming and low-efficiency. Particularly during the HF/HNO3 etching stage when dealing with granitic samples containing abundant feldspars and mica impurity minerals necessitates repeated treatments to eliminate feldspars completely; this not only increases etching cycles but also leads to sample loss significantly. It has a great impact on the application of in-situ cosmogenic nuclide dating in active tectonics. Consequently, physically separating quartz from samples before chemical purification can effectively shorten the chemical etching duration while the flotation separation method can effectively remove most gangue minerals in quartz and achieve preliminary purification of quartz.
This article presents a laboratory-integrated flotation purification device and proposes enhancements to the conventional quartz etching process in order to improve its purification efficiency. The purification device uses dodecylamine as the collector, hydrofluoric acid as the feldspar activator, nitric acid as the regulator, and eucalyptus oleanol as the foaming agent. The bubbling component within the device provides sufficient carbon dioxide bubbles to float out feldspar and other minerals in the sample reversely. To evaluate its efficacy in flotation separation, enrichment, and purification, this study conducted tests on two commonly encountered bedrock samples of granitic gneiss and quartzite.
Observation results under a stereomicroscope show that the quartz content in the quartz component after floating is more than 90%. The etching results of the whole rock and the floated quartz components show that after etching 2-3 times with HF/HNO3, the Al concentration can be reduced to less than 200ppm, which fully meets the requirement of cosmogenic nuclide dating. The quartz separated by flotation from cryptocrystalline quartzite samples can also reach the dating requirements after etching 7-8 times.
Compared to direct etching following bulk-rock sample crushing, this approach reduces etching time by over a half, significantly minimizing reagent consumption for HF/HNO3 etching and thereby enhancing TCND efficiency. The bubbling power section of our flotation device directly introduces carbon dioxide gas into the flotation liquid to increase the bubble content in the slurry. Consequently, there is improved collision and contact between quartz and feldspar particles with bubbles, resulting in enhanced flotation effectiveness. This system can be effectively employed for separating feldspar from other impurity minerals present in gneiss samples. The proposed flotation process in this study is straightforward and user-friendly while allowing flexibility in adjusting sample quantities ranging from tens to hundreds of grams as required. Furthermore, this high-efficiency flotation separation system may offer insights into processing zircon, apatite, and other dating samples.
It is difficult to use traditional trenching and field geological investigation to yield the age of paleoseismic events along active fault in western mountainous areas of China where the geomorphic trace mark and sediments are often eroded or altered by human activities. The recurrence interval of paleoearthquake possesses greater uncertainty. It is necessary to yield ages of paleoearthquake event from different ways and examine the reliability of paleoearthquake results. In these regions, an earthquake with magnitude greater than 7 can produce rock avalanches around 200~400km away from the epicenter, such as the Wenchuan earthquake in 2008, due to their structure setting of strong neotectonic activity and the higher topographic relief. Therefore, the seismic bedrock landslide and rock avalanche can record the occurrence time, intensity and damage of strong earthquake in the mountainous area. This provides a new way to assess the frequency and intensity of paleoearthquake occurring in the intraplate continental areas(such as the north-south seismic zone)where strong earthquakes recurred for hundreds to thousands of years based on the seismic landslide records. Identifying ancient earthquake bedrock collapse relics in Quaternary deposits and accurately determining their ages will not only help broaden the study on the recurrence history of active fault, but also assess the earthquake risk in mountainous area.As shown by previous studies, the Schmidt-hammer exposure-age dating(SHD)method is a relatively simple, rapid, cheap and non-destructive in-situ exposure age dating method. In this study, ancient earthquake bedrock landslides and rock avalanches with known historical records distributed on the Qinling northern piedmont fault and the Huashan piedmont fault are used to preliminarily establish the rock weathering factor with age calibration curve. The rebound values of rock surface at dozens of sampling sites of each rock avalanche and landslide are measured by Schmidt hammer and analyzed statistically. The weathering factor of the exposed rock of each rock avalanche and landslide is calculated and the solution of SHD method is discussed. The reliability of SHD is evaluated according to the measured data and the records of historical age. The main conclusions are as follows:(1)The Schmidt hammer rebound value of rock surface at three ancient earthquake bedrock landslides and rock avalanches is negatively correlated with their historical ages. The older the historical record age, the lower the average rebound value of the rock, and vice versa. Based on the statistical analysis of weathering factors of rocks of bedrock landslides and rock avalanches, a preliminary age calibration curve is obtained as T=(19 723±888)×fw-(2 145±166). This curve can be used to infer the bedrock landslides and rock avalanches of more than 5×102 a BP, and it provides a new relative dating method for the ancient bedrock landslide and rock avalanches within the age of 3 000a BP in the northern margin of the Qinling Mountains.(2)Under the climatic and lithological conditions of the northern margin of the Qinling Mountains, the relative ages of bedrock landslide and rock avalanches can discriminate the interval of millennium scale according to the rock rebound value measured by Schmidt hammer. However, it cannot distinguish the difference in weathering degree of the bedrock landslide and rock avalanches with the interval of less than 500 years.(3)The Schmidt hammer rebound value measured repeatedly on fresh rocks shows that the fluctuation range of the rebound values is small, within the value of 0-3, which is helpful to rapidly select qualified sampling sites for terrestrial in-situ cosmogenic nuclide dating(TCND). Thus, the Schmidt hammer value can be used to evaluate whether the rock samples have the problem of nuclide inheritance induced by complex exposure history such as post-exposure and secondary transportation. This would introduce greater objectivity to the sample selection and possibly require less samples, thus reducing the costs; meanwhile, it will improve the dating efficiency and ensure the reliability of TCND. Therefore, SHD method is a valuable complementary method to TCND.(4)Under the climatic and lithological conditions in the northern margin of the Qinling Mountains, the rebound value decreases by (25%±1%) for rocks after weathering for 2ka, by (16%±1%) for 1ka, and by (15%±1%) for 0.5ka.
The Karakoram Fault is located in the west of the Qinghai-Tibet Plateau and crosses Kashmir, Xinjiang and Tibet in China. It is a large normal dextral strike-slip fault in the middle of the Asian continent. As a boundary fault dividing the Qinghai-Tibet Plateau and the Pamir Plateau-Karakoram Mountains, the Karakoram Fault plays a role in accommodating the collision deformation between the Indian plate and the Eurasian plate and in the tectonic evolution of the western Qinghai-Tibet Plateau. The fault trace in Ngari area is clear and the faulted landforms are obvious, which show strong activity characteristics in late Quaternary. As a large active fault, only one earthquake of magnitude 7 has been recorded on the Karakoram Fault since the recorded history, namely, the Tashkurgan earthquake of 1895 at its north end. There are no records of strong earthquakes of magnitude≥7 along the rest of the fault, and no paleo-seismic research has been carried out. Ages of recent strong earthquake activity and earthquake recurrence intervals are not clear, which greatly limit the accuracy of seismic risk assessment. In this study, we investigated the fault geometry and faulted landforms in Ngari area, collected OSL samples of the faulted landforms and sag ponds in Zhaxigang, Menshi and Baga towns and preliminarily discussed the ages of recent strong earthquake activity.
Study shows that the fault can be divided into three sections by Zhaxigang town and Suoduo village, and the structure and properties of each section are significantly different. In west Zhaxigang town section, the fault is dominated by dextral strike-slip with certain vertical movement, it is almost straight on the surface, with river terraces, alluvial-proluvial fans and water system faulted ranging from tens to hundreds of meters. In Zhaxigang town to Suoduo village section, the normal faulting is remarkable, the main fault constitutes the boundary fault between Ayilari Mountain and Gar Basin; fault facets and fault scarps are common along the fault line, there are also secondary faults with the same or opposite dip as the main fault developed near the piedmont basin. In east Suoduo village section, the main part of the fault is located at the south foot of Gangdise Mountain, and in addition to the piedmont fault, several approximately parallel faults are also developed on the southern alluvial-proluvial fans and moraine fans which are mainly dextrally faulted with certain vertical component.
According to the analysis of the faulted landforms and dating of the OSL samples collected from the sag ponds and faulted landforms in the west of Zhaxigang town, the east of Menshi town and the east of Baga town, the ages of recent strong earthquake activity on the fault are analyzed as follows. In the west of Zhaxigang town, the age of recent strong earthquake activity of the fault is constrained to be close to 2.34kaBP according to the average OSL dating results of KKF-3 and KKF-4. In the east of Menshi town, the recent earthquake activity age of fault f2 is 4.67~3.01kaBP, but closer to 3.01kaBP according to the OSL dating results of KKF-11 of the youngest faulted geomorphic surface and average OSL dating results of KKF-6 and KKF-13 collected from sag ponds. In the area near Angwang village, Baga town, it is inferred that the recent strong earthquake activity age of the fault is close to 2.54kaBP according to the OSL dating results of KKF-2 collected from sag pond. If the faults of above three places are active at the same time, the age of recent strong earthquake activity of the fault is close to 2.63kaBP. The Karakorum Fault in Ngari area has obvious segment boundaries, and the activity of each segment and in its internal branch faults is most likely to be independent.
The earthquake recurrence interval on the fault is estimated to be 2.8ka according to the slip rate and the amount of displacement. From the above analysis, it can be seen the time since the last strong earthquake activity of Karakorum Fault may have been very close to the interval of earthquake recurrence. If the fault is characterized by a quasi-periodic in-situ recurrence, the energy accumulation in the fault may have reached a very high degree and the risk of recurrence of strong earthquake events of the fault may be very high, so more attention should be paid and more detailed research on the paleo-earthquake events and recurrence intervals should be carried out as quickly as possible.
Over the last two decades, in-situ cosmogenic 14C dating has become an import tool in Quaternary geology and is recognized to geoscientists because of its potential to provide information on exposure age and process rate estimates for geomorphic studies. The in-situ cosmogenic radiocarbon has a relatively short half-life(5730 yr)and is substantially more sensitive than all the other cosmogenic nuclides used so far. It is therefore particularly useful to determine surface-exposure ages of Holocene landforms and quantify erosion rates in rapidly denuding landscapes during the past few tens of thousands of years. Moreover, in situ 14C is produced in quartz which is both highly resistant to weathering and common in nature, so it can be used in combination with other in-situ cosmogenic nuclides such as 3He, 10Be,21Ne,26Al, and 36Cl to constrain complex exposure histories involving burial and/or erosion occurring over the past 25ka. The age and slip rate of Holocene normal fault have been undoubtedly a challenge for seismologists to be faced with as result from lack of appropriate late Quaternary sediment. Recently, the cosmogenic nuclides such as 36Cl of preserved, seismically exhumed normal fault scarps were used to identify the last few major earthquakes and recover their ages and displacements through the modeling of the content of 36Cl in the scarp rocks. This paper mainly summarizes the development of in-situ 14C dating, including its research history, production rate estimate, production mechanism, chemical behavior and experimental method. The potential application of in-situ 14C dating to recovering past earthquakes, their timing, and the regularity of their recurrence for preserved, seismically exhumed normal fault scarps is also introduced.
The fluvial terrace has plenty of paleoclimate and paleoenviromental information which play an important role in paleoclimate and paleoenviromental researches.In this paper,we drilled a 42.85m-long core(N06S2)in 2007,which was located in the south bank of Yangtze River at Shifuqiao in Qixia district of Nanjing City.Firstly,fine quartz grains(4~11μm)were extracted from bulk samples in dark room,and the quartz purity tests were conducted.The results show that purity can satisfy the experiment.All measurements were performed on an automated Daybreak 2200 TL/OSL system with blue(470±5nm)light stimulation and U-340 luminescence detection filters.Thick source alpha counting(TSAC)was used to measure the uranium and thorium concentrations.The potassium content was determined using flame spectrophotometer.Secondly,the preheat plateau test and dose recovery test were performed on one sample using the SAR protocol.The results indicate that the fast component dominates the OSL signals.In preheat plateau test,identical De in the thermal treat from 160~260℃ was observed,thus we use the preheat temperature of 220℃ for 10 seconds.The recuperation ratios of zero point are below 2%and the recycling ratios lie between 0.9 and 1.1.In dose recovery test,OSL signal sensitivity changes are well corrected.Tests of luminescence characteristics confirm the suitability of the material for OSL dating.At last,samples from this drilling core were systematically dated by optically stimulated luminescence(OSL)dating method,and samples which contain organic matters were dated by AMS14 C.The results show that the De values from the two methods accord with each other very well.However,OSL dating results show that there is a hiatus in this core,and the hiatus,which ranges from 1.9ka to 7.9ka,may be the result of change of Yangtze River's channel or the erosion of the river.The ages of the fluvial deposition mainly range from 0.26ka to 1.9ka and 7.9ka to 9.1ka,it could be attributed to the results of paleoclimate and sea levels change.Meanwhile,study results on pollen and spores show that the paleoclimate has changed from warm wet to temperate wet during the stage of hiatus.
This paper presents a comparison of the calendar range of individual paleoearthquake calculated by conventional calibration,Bayesian analysis of series of peat samples as well as depth-age wiggle matching.The results suggest that: (1)The Bayesian analysis provides an excellent means to enhance chronological resolution when applied to a series of radiocarbon dates from sections with clear stratigraphic relationships.Such application can assess systematic errors when combined with independent chronological information,and determine the optimum chronological information for specific events and contexts.(2)The calendar ranges of series of samples collected from the same peat but different sampling thickness were compared with that of depth-age wiggle matching.The result shows that the chronological resolution by depth-age wiggle matching for the peat sample with thickness less than 2cm could achieve less than 100a.Therefore,the condition to obtain a high resolution calendar age is to have 5~6 samples with 0.5~2cm sampling thickness each and the interval of samples is 0.5~1cm.(3)The calendar range of paleoearthquakes constrained by the Markov chain Monte Carlo(MCMC)Bayesian analysis model,which constructs the order of samples according to their position in the strata with series of radiocarbon dates,was compared with calendar range by the conventional method.The results show that Bayesian analysis could obtain high-precision calendar dates for closely spaced samples.(4)Therefore,the calendar interval of the paleoearthquake event on the middle segment of Huaiyuan Fault was inferred as 1340~1114cal a BP(2σ)by the above systematical comparsion.
More than ten volcanoes of Jingpohu Holocene Volcanic Group consist of five small eruption centers situated at southwest area and northeast area separately. Southwest area includes four eruption centers, namely “Crater Forest”, “Daganpao”, “Wudaogou” and “Mihunzhen”, respectively. Northeast area has only one eruption center called “Hamatang”. Eruptive materials include mainly lava flow, splash deposit and airfall deposit. Volcanic cone consists of cinder, bomb, driblet and thin lava flow. The thickness of a
Recent magnetostratigraphic and lithostratigraphic studies in the western Tarim basin have led to better constrained depositional and deformational histories. As a lithostratigraphic unit, the Xiyu Formation consists an abruptly upward-coarsening fanglomerate locally interbedded with lenticular sandstone and sandy mudstone beds. It is unconformably or disconformably overlain by the Wusu formation. The concordantly underlying Atushi Formation is predominately fluvial siltstones, sandy mudstones, and rippled
A comprehensive study of chronology for the lower terraces along several major rivers in the Yanhuai basin and its adjacent areas is made by TL,IRSL and 14C dating as well as the Spore-pollen analysis method. The deposited ages of sediments heve been dated and the formation times of the geomorphic surfases for these lower terraces are estimated. The results show that the lower terraces in this region are associated with the regional motion and the climate conditions since late Pleistocene time